摘要:This research aims to elucidate the crystallinity, structural and mechanical properties of cotton/spandex knitted fabric after conducting heat setting i.e., annealing process with optimized condition for the first time. Experimental results disclosed that, crystallinity index (CI) (%) of heat-treated cotton/spandex were increased with increased temperature and also mechanical properties i.e., tensile strength was improved as the temperature rose from 120 to 140°C and decreased with augmenting temperature ranges, which is in good agreement with the findings of CI % through X-ray diffraction (XRD) patterns. The attendance of cellulose dehydration was further confirmed by Fourier transform infrared (FT-IR) spectra in order to observe the structural integrity.