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  • 标题:Refined separation of combined Fe–Hf from rock matrices for isotope analyses using AG-MP-1M and Ln-Spec chromatographic extraction resins
  • 本地全文:下载
  • 作者:Ting Cheng ; Oliver Nebel ; Paolo A. Sossi
  • 期刊名称:MethodsX
  • 印刷版ISSN:2215-0161
  • 电子版ISSN:2215-0161
  • 出版年度:2014
  • 卷号:1
  • 页码:144-150
  • DOI:10.1016/j.mex.2014.08.004
  • 语种:English
  • 出版社:Elsevier
  • 摘要:Graphical abstractAbstractA combined procedure for separating Fe and Hf from a single rock digestion is presented. In a two-stage chromatographic extraction process, a purified Fe fraction is first quantitatively separated from the rock matrix using AG-MP-1M resin in HCl. Hafnium is subsequently isolated using a modified version of a commonly applied method using Eichrom LN-Spec resin. Our combined method includes:•Purification of Fe from the rock matrix using HCl, ready for mass spectrometric analysis.•Direct loading of the matrix onto the resin that is used for Hf purification.•Collection of a Fe-free Hf fraction.
  • 关键词:Fe–Hf separation;AG-MP-1M resin;Ln-Spec resin
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