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  • 标题:Precision test for spectral characteristic of NIR spectroscopy and bomb calorimeter for measuring higher heating value of Leucaena Leucocephala
  • 本地全文:下载
  • 作者:Jetsada Posom ; Panmanas Sirisomboon ; Wanphut Saechua
  • 期刊名称:MATEC Web of Conferences
  • 电子版ISSN:2261-236X
  • 出版年度:2018
  • 卷号:192
  • DOI:10.1051/matecconf/201819203049
  • 语种:English
  • 出版社:EDP Sciences
  • 摘要:The higher heating value (HHV) plays a significant role in determining of the energy potential of biomass. The method to receive this value using a bomb calorimeter takes a long time approximately of 15 minutes. The implementation of near infrared spectroscopy (NIR) technique by generating a prediction model can be replaced the former method in order to reduce time into 2 minutes. Therefore, the precision of both techniques have to be concerned in order to get the reliable values. The repeatability and reproducibility processes were carried out to evaluate the precision of both methods. It was found that the percentage difference of standard deviation (SD) from the mean of repeatability for the NIR was less than 5 % and for reproducibility was slightly over 5 % (but not over than 10%). The SD of repeatability and reproducibility of the bomb calorimeter were 54.6 J/g (0.3 % difference of average HHV value) and 81.3 J/g (0.5 % difference of average HHV value) respectively. The average HHV from the bomb calorimeter was 18,166.77±236.29 J/g. Both techniques showed very low percentage difference of the SD from the mean that revealed very high reliability and precision of measurements.
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