期刊名称：Current Journal of Applied Science and Technology
印刷版ISSN：2457-1024
出版年度：2016
卷号：15
期号：2
页码：1-9
语种：English
出版社：Sciencedomain International
摘要：The purpose of this paper is study the preparation “in situ” of magnesium–tantalum phases when reacted with oxygen and hydrogen during a mechanical milling process. Different phases were formed as function of the milling time. High energy ball milling was utilized to prepare hydrogenated compounds by controling the milling between 5 and 20 hours with a ball powder weight ratio of 10 and using methanol as the control agent. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) were used to characterize the compounds. The XRD results at 20 h of milling revealed that only hydrogenated species (Ta2H and TaH0.5) and Mg(OH)2 were present.
关键词：Tantalum hydrides;high energy ball milling;solvent dissociation;XRD;SEM
