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  • 标题:In situ synchrotron‐based X‐ray powder diffraction and micro‐Raman study of biomass and residue model compounds at hydrothermal conditions
  • 作者:Morgan L. Thomas ; Ian S. Butler ; Janusz A. Kozinski
  • 期刊名称:Energy Science & Engineering
  • 电子版ISSN:2050-0505
  • 出版年度:2015
  • 卷号:3
  • 期号:3
  • 页码:189-195
  • DOI:10.1002/ese3.68
  • 语种:English
  • 出版社:John Wiley & Sons, Ltd.
  • 摘要:

    Abstract

    The applications of synchrotron X‐ray powder diffraction ( XRPD ) and laser micro‐Raman techniques in an examination of the dissolution, transformation, and gasification of pure cellulose and models for biomass residue under hydrothermal conditions in a diamond‐anvil cell are reported. The results contribute to the measurement of in situ time‐resolved profiles of biomass reactions, catalyst stability, and residue formation that occur in aqueous fluids at near‐ and supercritical conditions.

    The applications of synchrotron X‐ray powder diffraction (XRPD) and laser micro‐Raman techniques in an examination of the dissolution, transformation and gasification of pure cellulose and models for biomass residue under hydrothermal conditions in a diamond‐anvil cell are reported. The results contribute to the measurement of in situ time‐resolved profiles of biomass reactions, catalyst stability and residue formation that occur in aqueous fluids at near‐ and supercritical conditions.

  • 关键词:Biomass; diamond‐anvil cell; hydrothermal; Raman; supercritical water; X‐ray diffraction
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