摘要：Highlights•Small-gap-smooth-cup-and-bob is suitable geometry for dilute digested sludge (~2%).•Small-gap-vane-and-rough cup is preferred for sludge at medium thickness (~3.5%).•Roughened wide gap geometry is preferred for highly thickened digested sludge (~6%).•An equilibrium time at each point of flow curve is necessary for sludge measurement.•Flow curve data requires to visually inspected for instabilities.AbstractInconsistent experimental procedures have been used to characterize sludge rheology in literature. This often has resulted in proposing different rheological models for sludge as well as non-comparable data. Any collected rheological data needs to be interpreted considering the methodology used for its collection because otherwise they cannot be used by engineers for design and troubleshooting. This paper intends to shed light on the influential parameters during data collection procedure to produce a reliable and reproducible data.This paper systematically investigates the impact of different geometries, preshear, equilibrium, rest and storage time on flow curve measurement for digested sludge in the range of 2.3 to 6% total solid and recommends a reliable procedure for reproducible sludge flow curve measurements. While the magnitude of impacts is different, we found all factors are significantly dependent on the sludge solid concentration. Besides, the method of the development of the protocol can be utilized to develop appropriate protocols for rheological characterization of any other sludge. The customization highlights are:•Selecting the geometry according to the sludge solid concentration.•Allocating an equilibrium time at each point of flow curve according to the sludge solid concentration.•Flow curve data requires to visually inspected for instabilities.Graphical abstractDisplay Omitted
