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  • 标题:Effect of Microwave Irradiation on Oximation of Acetylferrocene
  • 本地全文:下载
  • 作者:Yutaka Okada ; Ryuichi Maeda
  • 期刊名称:Green and Sustainable Chemistry
  • 印刷版ISSN:2160-6951
  • 电子版ISSN:2160-696X
  • 出版年度:2021
  • 卷号:11
  • 期号:1
  • 页码:1-8
  • DOI:10.4236/gsc.2021.111001
  • 语种:English
  • 出版社:Scientific Research Publishing
  • 摘要:Microwave-assisted reactions are an environmentally friendly approach for synthesizing organic compounds. In this study, oximation of acetylferrocene and acetophenone was conducted under both microwave irradiation and conventional heating conditions. Acetylferrocene and acetophenone were subjected to oximation under the two conditions in various solvent mixtures, and the extent of conversion was determined by 1H nuclear magnetic resonance spectroscopy. Microwave irradiation was found to accelerate the rate of oximation of both acetylferrocene and acetophenone. Acceleration of the reaction under microwave irradiation was attributed to the efficient absorption of microwaves by the ferrocene nucleus.
  • 关键词:Microwave Irradiation;Conventional Heating;Ferrocene Nucleus;Acetophenone;Acetylferrocene;Oximation
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