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  • 标题:Optimization of the Pre-treatment Method for the Determination of 9 Organophosphorus Pesticide Residues in Cabbage by Gas Chromatography
  • 本地全文:下载
  • 作者:Siya Guo ; Xiaoyan Wang ; Zongyi Zhang
  • 期刊名称:E3S Web of Conferences
  • 印刷版ISSN:2267-1242
  • 电子版ISSN:2267-1242
  • 出版年度:2021
  • 卷号:299
  • 页码:1-7
  • DOI:10.1051/e3sconf/202129902012
  • 语种:English
  • 出版社:EDP Sciences
  • 摘要:The purpose of this study was to optimize the pre-treatment process for the detection of 9 organophosphorus pesticide residues in cabbage by gas chromatography, and to conduct a comparative experiment between this method and the standard method NY/T 761-2008 of the Ministry of Agriculture. The results show that the optimized pre-treatment method is to use 10 mL acetonitrile as the extractant, 150 mg N-propyl ethylenediamine (PSA) and 15 mg graphitized carbon black (GCB) as the purification agent, which can reduce the use of extractant and inorganic salt in the pre-treatment process, increase the recovery and detection limit, reduce the matrix effect and cost of instrument maintenance.
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