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  • 标题:Volatile component profiles of conventional and lactose-hydrolyzed UHT milk—a dynamic headspace gas chromatography-mass spectrometry study
  • 作者:Therese Jansson ; Sidsel Jensen ; Nina Eggers
  • 期刊名称:Dairy Science & Technology
  • 印刷版ISSN:1958-5586
  • 电子版ISSN:1958-5594
  • 出版年度:2014
  • 卷号:94
  • 期号:4
  • 页码:311-325
  • DOI:10.1007/s13594-014-0164-7
  • 语种:English
  • 出版社:EDP Sciences
  • 摘要:

    Lactose-hydrolyzed milk gains still increasing market share, and understanding the chemical characteristics of lactose-hydrolyzed milk products is important for the dairy industry. The aim of the present study was to identify and compare volatile compounds of commercial lactose-hydrolyzed and conventional ultra-high temperature (UHT) milk. For this purpose, the volatile compounds of lactose-hydrolyzed (<1% lactose), conventional (100% lactose), and filtered (60% lactose) UHT-treated milk were extracted using dynamic headspace sampling and analyzed by gas chromatography-mass spectrometry (GC-MS). A total of 24 volatile compounds were identified including ketones, aldehydes, and sulfides. Overall, principal component analysis (PCA) showed grouping of the different milk types, with loadings indicating a higher concentration of ketones in conventional versus lactose-hydrolyzed UHT milk, but PCA also indicated a marked batch-to-batch variation. Elucidation of individual volatile compounds detected also revealed that the content of ketones in general was higher in conventional UHT milk than in lactose-hydrolyzed milk; however, no significant differences in the volatile compound profiles could be identified between the various milk types as a result of the batch-to-batch variation. The present study highlights a useful analytical method based on dynamic headspace sampling and GC-MS to profile volatiles important for the flavor characteristics of lactose-hydrolyzed and conventional UHT milk. In addition, the present study reveals that a considerable batch-to-batch variation exists in industrially produced batches of lactose-hydrolyzed UHT milk, which must be considered an important challenge for the dairy industry.

  • 关键词:Lactose-hydrolyzed milk ;UHT ;Milk batch variations ;Dynamic headspace sampling ;GC-MS
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