期刊名称：International Journal of Fundamental and Applied Sciences
印刷版ISSN：2278-1404
出版年度：2012
卷号：1
期号：2
页码：30-33
出版社：BioMedAsia
摘要：Background and Aim: A new series of macrocyclic compounds 1-4 have been synthesized using tin as templates. Method:Tin templates are formed by refluxing the solution of dibutyltin (IV) oxide with orthophenylenediamine (L1H), 4-chlorocatechol (L2H), butane dithiol (L3H) and 3-carboxypropyldisulphide (L4H). Results:The reaction is visualized by cleavage X-Sn-X (X= oxygen/ nitrogen/ sulphur atom) bond of tin template when treated with adipoyldichloride. Conclusion:The compounds 1-4 are characterized with the aid of elemental analyses, IR and NMR (1H, 13C) studies which confirmed their proposed framework.
