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  • 标题:Electrochemical Reduction of 2-Methylcyclohexane-1, 3-Dione at Stainless Steel (Ss-316) Electrode in Basic Media
  • 本地全文:下载
  • 作者:Sushil K. Sharma ; Geeta Wadhvani ; I. K. Sharma
  • 期刊名称:International Journal of Innovative Research in Science, Engineering and Technology
  • 印刷版ISSN:2347-6710
  • 电子版ISSN:2319-8753
  • 出版年度:2014
  • 卷号:3
  • 期号:12
  • 页码:17837
  • DOI:10.15680/IJIRSET.2014.0312013
  • 出版社:S&S Publications
  • 摘要:Cyclic voltammo grams of 2-Methylcyclohexane-1, 3-dione were recorded at different pH (4.0, 7.0, & 9.0) to establish the optimum conditions its the reduction. The Galvanostatic reduction of 2-methylcyclohexane-1, 3 - dione was thereafter carried out galvanostatically at pH = 9.0 using Stainless Steel (SS -316) as a working electrode. The good yield (88.8%), of 3-hydroxy-2-methyl cyclohexanone was obtained, which was isolated and purified by chromatographic techniques and characterized on the basis of spectral analysis.
  • 关键词:2-Methylcyclohexane-1; 3-dione; Galvanostatic reduction; Stainless Steel (SS-316) Electrode; Cyclic ; Voltammetry
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