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  • 标题:Gas–liquid chromatography of hyocholic acid
  • 本地全文:下载
  • 作者:Glen E. Mott ; Richard W. Moore ; Raymond Reiser
  • 期刊名称:JLR Papers In Press
  • 印刷版ISSN:0022-2275
  • 电子版ISSN:1539-7262
  • 出版年度:1971
  • 卷号:12
  • 期号:1
  • 页码:117-119
  • 语种:English
  • 出版社:American Society for Biochemistry and Molecular Biology
  • 摘要:Partial derivatives of hyocholic acid were formed under the usual conditions for trifluoroacetylation of bile acids (trifluoroacetic anhydride, 35°C for 20 min). Complete trifluoroacetylation of hyocholic acid was achieved at 80°C for 30 min, or at 60°C for 30 min when a trace of pyridine was added to the reaction mixture.
  • 关键词:bile acids ; methyl esters ; trifluoroacetylation ; partial derivatives ; steric hindrance ; pyridine
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