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  • 标题:A method for the rapid qualitative and quantitative analysis of 4,4-dimethyl sterols
  • 本地全文:下载
  • 作者:G. F. Gibbons ; K. A. Mitropoulos ; Kalpana Ramananda
  • 期刊名称:JLR Papers In Press
  • 印刷版ISSN:0022-2275
  • 电子版ISSN:1539-7262
  • 出版年度:1973
  • 卷号:14
  • 期号:5
  • 页码:589-592
  • 语种:English
  • 出版社:American Society for Biochemistry and Molecular Biology
  • 摘要:A simple and relatively rapid technique has been developed for the separation of several 4,4-dimethyl steryl acetates, some of which contain sterically hindered nuclear double bonds. The method involves thin-layer chromatography on silver nitrate-impregnated silica gel and silver nitrate-impregnated alumina. The separated steryl acetates may then be analyzed quantitatively by gas–liquid chromatography.
  • 关键词:thin-layer chromatography ; silica gel–silver nitrate ; alumina–silver nitrate ; gas–liquid chromatography
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