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  • 标题:A convenient synthesis of 3-keto bile acids by selective oxidation of bile acids with silver carbonate-Celite.
  • 本地全文:下载
  • 作者:K Y Tserng
  • 期刊名称:JLR Papers In Press
  • 印刷版ISSN:0022-2275
  • 电子版ISSN:1539-7262
  • 出版年度:1978
  • 卷号:19
  • 期号:4
  • 页码:501-504
  • 语种:English
  • 出版社:American Society for Biochemistry and Molecular Biology
  • 摘要:A number of 3-keto bile acids were synthesized by the selective oxidation of bile acid methyl esters with silver carbonate-Celite in refluxing toluene. The pure 3-keto bile acids were isolated simply by filtering the reaction mixture and concentrating the filtrate. The relation of the bile acid structure to the oxidation rate is also discussed.
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