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  • 标题:Alphacypermethrin residues in milk following a pour-on treatment in buffaloes
  • 作者:Giorgio Smaldone ; Raffaele Marrone ; Claudia Chirollo
  • 期刊名称:Italian Journal of Food Safety
  • 电子版ISSN:2239-7132
  • 出版年度:2013
  • 卷号:2
  • 期号:2
  • 页码:19
  • DOI:10.4081/ijfs.2013.e19
  • 语种:English
  • 出版社:PAGEPress Publications
  • 摘要:Aim of this study was to detect and quantify the residues of alphacypermethrin (ACYP), a pyrethroid insecticide, in buffalo milk. Ten animals were treated pour-on at the manufacturer’s recommended cattle dose. Milk samples were collected from each animal before treatment, every 12 h for the first three days (12, 24, 36, 48, 60, 72 h) and once on day 5 after treatment. Milk samples were subsequently analysed by ultraperformance liquid chromatography coupled with tandem mass spectrometry (UPLC-MS/MS). All samples showed levels of ACYP above the maximum residual limit of 20 ppb established for bovine milk.
  • 关键词:Alphacypermethrin; Buffaloes; Milk; Pour-on treatment
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