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  • 标题:Direct Quantitative Analysis of Respirable Cristobalite on Filter by Infrared Spectrophotometry
  • 本地全文:下载
  • 作者:Yasushi SHINOHARA
  • 期刊名称:Industrial Health
  • 印刷版ISSN:0019-8366
  • 电子版ISSN:1880-8026
  • 出版年度:1996
  • 卷号:34
  • 期号:1
  • 页码:25-34
  • DOI:10.2486/indhealth.34.25
  • 出版社:National Institute of Occupational Safety and Health
  • 摘要:A direct on-filter method in infrared spectrophotometry was investigated for the quantitative analysis of respirable cristobalite. A polypropylene membrane filter was employed for this analysis, because the membrane filter has high transparency and no interference peak in the spectral range to be used (750-250cm-1). Linear relation between the sample weight and peak height (absorbance) for three specific peaks at 620, 385 and 300cm-1 of cristobalite were confirmed over the range from 45 to 1, 000μg/cm2 for 620 cm-1 peak and 45-2, 380μg/cm2 for 385 and 300cm-1 peaks. The variation of absorbance with the difference of particle size was smaller in filter sample than in potassium bromide pellet sample. As a conclusion, this direct on-filter method can be used for quantitative analysis of cristobalite in airborne dust in working environment.
  • 关键词:Cristobalite;Silica mineral;Infrared spectrophotometry;Membrane filter;Quantitative analysis;Particle size effect
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