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  • 标题:ヒト血液中からの農薬カルタップの抽出
  • 本地全文:下载
  • 作者:三井 利幸 ; 藤村 義和
  • 期刊名称:Journal of Health Science
  • 印刷版ISSN:1344-9702
  • 电子版ISSN:1347-5207
  • 出版年度:1986
  • 卷号:32
  • 期号:4
  • 页码:305-307
  • DOI:10.1248/jhs1956.32.305
  • 出版社:The Pharmaceutical Society of Japan
  • 摘要:The selection of best solvent for extracting cartap from human blood was examined. The experimental procedures were as follows ; One ml of blood sample was added to 0.5 ml of 8% sodium hydroxide solution in a 15 ml test tube. The sample was extracted with 5 ml of cyclohexane by shaking for 3 min, and centrifuged at 3000 rpm for 2 min. The cartap extracted with cyclohexane was derivatized by reacting with 3, 4-dimethyl benzyl chloride. The 3, 4-dimethyl benzyl derivative of cartap was spectrophotometrically measured by using tropaeoline OO as an ion-associating reagent. For the extraction of cartap from blood sample no interference could be observed with the compounds, such as Fe (III), Cu (II), glycine, L-phenylalanine, urea, glucose, lactose.
  • 关键词:agricultural chemical cartap;human blood;spectrophotometric determination
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