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  • 标题:流動パラフィン処理既製アビセルSF薄層プレートを用いた有機水銀ジチゾネートの分析
  • 本地全文:下载
  • 作者:石倉 俊治 ; 与那覇 政憲 ; 須永 糸子
  • 期刊名称:Journal of Health Science
  • 印刷版ISSN:1344-9702
  • 电子版ISSN:1347-5207
  • 出版年度:1972
  • 卷号:18
  • 期号:4
  • 页码:281-283
  • DOI:10.1248/jhs1956.18.281
  • 出版社:The Pharmaceutical Society of Japan
  • 摘要:An analytical method is described for the detection of inorganic mercury, alkylmercury, alkoxyethylmercury, and phenylmercury dithizonates on commercially available Avical SF thin-layers coated with liquid paraffin. The compounds examined were distinctly separated with high reproducibility of Rf values. From biological samples to which mercuric compounds were added as a chloride, the compounds were isolated as the dithizonates by extraction of the samples with dithizone-carbon tetrachloride solution and subsequently the dithizonates were purified by column chromatography using alumina. When the dithizonates were applied to reverse-phase thin-layer chromatography, the compounds were detected even at a low level.
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