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  • 标题:高速液体クロマトグラフィーによる乳液, クリーム中の没食子酸プロピルの定量法
  • 本地全文:下载
  • 作者:鎌田 国広 ; 風間 成孔
  • 期刊名称:Journal of Health Science
  • 印刷版ISSN:1344-9702
  • 电子版ISSN:1347-5207
  • 出版年度:1984
  • 卷号:30
  • 期号:6
  • 页码:390-392
  • DOI:10.1248/jhs1956.30.6_390
  • 出版社:The Pharmaceutical Society of Japan
  • 摘要:A high performance liquid chromatographic (HPLC) method was developed for determining propyl gallate (PG) in cosmetic lotions and creams. The sample is extracted with ethyl acetate, and the extract is cleaned up on a florisil column. PG in the purified extract is determined by reverse phase HPLC on a octadecylsilated silica column using a mobile phase of acetonitrile-water with 5% acetic acid, UV detector (275 nm) for the detection. Recoveries of PG from cosmetic samples spiked at 0.005 and 0.001% leveles were 96.2-98.0%, and the coefficients of variation were within 2.71-3.81%.
  • 关键词:HPLC;propyl gallate;antioxidant;cosmetic;propyl gallate determination;florisil column
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