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  • 标题:環境中の塩化ビニールモノマーの定量
  • 本地全文:下载
  • 作者:田中 克彦 ; 深谷 勝久 ; 西山 信一
  • 期刊名称:Journal of Health Science
  • 印刷版ISSN:1344-9702
  • 电子版ISSN:1347-5207
  • 出版年度:1977
  • 卷号:23
  • 期号:1
  • 页码:48-53
  • DOI:10.1248/jhs1956.23.48
  • 出版社:The Pharmaceutical Society of Japan
  • 摘要:A procedure for determination of a micro-amount of vinyl chloride monomer in environment is described. In this method, a modified concentration tube containing fire brick C-22 and 5% PEG 400 on Chromosorb WAW was used. The tube was cooled with Dry Ice methanol and sample gases collected in a sampling bag from atmosphere or evaporated from water by aeration was passed through the tube. Vinyl chloride monomer and other organic gases were condensed on the fire brick C-22. Temperature of the tube was raised to room temperature and vinyl chloride monomer was introduced into a gas chromatograph, by which a greater part of other organic gases remained on the 5% PEG 400 on Chromosorb WAW. By this procedure, as little as 0.3 ppb of vinyl chloride monomer in 1 liter of atmospheric air, 0.01 ppb of vinyl chloride monomer in 100 ml of water can be determined without interference of co-existing organic substances.
  • 关键词:vinyl chloride monomer;gas chromatography;cold trapping;atmosphere;water;adsorption column;micro determination
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