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  • 标题:固相抽出法による水中農薬の一斉分析における酢酸エチルの利用
  • 本地全文:下载
  • 作者:大橋 則雄 ; 土屋 悦輝 ; 笹野 英雄
  • 期刊名称:Journal of Health Science
  • 印刷版ISSN:1344-9702
  • 电子版ISSN:1347-5207
  • 出版年度:1994
  • 卷号:40
  • 期号:3
  • 页码:292-297
  • DOI:10.1248/jhs1956.40.292
  • 出版社:The Pharmaceutical Society of Japan
  • 摘要:The application of ethyl acetate as the elution solvent for solid-phase extraction (SPE) of 34 organic pesticides in drinking water was evaluated using octadecyl (C18) bonded porous silica, octyl (C8) bonded porous silica and styrene divinyl benzene copolymer (PS-1) cartridges. A 500 ml volume of drinking water spiked with 0.5 μg of each pesticide was passed through each cartridge, absorbed target pesticides were eluted with 2 ml of ethyl acetate and analyzed using capillary gas chromatography-mass spectrometry. Target pesticides except for captan could be detected at 0.2-0.52μg/l level from each cartridge, it was confirmed that ethyl acetate was a suitable solvent as the eluent.
  • 关键词:pesticide;solid phase extraction;determination;elution solvent;tap water;GC/MS
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