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  • 标题:Secondary Ionization Mass Spectrometry-Linked Scanning Analysis for Identification of Aloenin in Foods Containing Aloe arborescens MILLER
  • 本地全文:下载
  • 作者:MASATOSHI YAMAMOTO ; KIYOSHI SUGIYAMA ; MASAMI YOKOTA
  • 期刊名称:Journal of Health Science
  • 印刷版ISSN:1344-9702
  • 电子版ISSN:1347-5207
  • 出版年度:1992
  • 卷号:38
  • 期号:4
  • 页码:324-328
  • DOI:10.1248/jhs1956.38.324
  • 出版社:The Pharmaceutical Society of Japan
  • 摘要:Secondary ionization mass spectrometry (SIMS)-linked scanning analysis was used as a method for identifying a specific Aloe arborescens MILLER (Kidachi-aroe) component, aloenin, in health foods containing Kidachi-aroe. The compound was extracted with methanol and identified in positive mode and constant B/E using SIMS-linked scanning analysis without any further purification such as a chromatography. Kidachi-aroe was detected in the sample using aloenin as an indicator. In the SIMS-linked scanning spectra of health foods containing Kidachi-aroe, peaks were observed of a quasi-molecular ion (m/z 411[M+H]+) and its daughter ion at m/z 249, indicating the structure of aloenin. Kidachi-aroe was thus detected when present in health foods. The proposed method is easy, rapid and accurate for both characterization and estimation of aloe materials in health foods containing Kidachi-aroe.
  • 关键词:health food containing aloe;Aloe arborescens MILL. Kidachi-aroe;secondary ionization mass spectrometry (SIMS)-linked scanning spectrum;identification test;aloenin
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