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  • 标题:空気中の塩素測定法における各種捕集剤の検討とシアン化カリウム中の不純物質の同定
  • 本地全文:下载
  • 作者:広瀬 義文 ; 森本 功 ; 興津 知明
  • 期刊名称:Journal of Health Science
  • 印刷版ISSN:1344-9702
  • 电子版ISSN:1347-5207
  • 出版年度:1990
  • 卷号:36
  • 期号:4
  • 页码:277-282
  • DOI:10.1248/jhs1956.36.277
  • 出版社:The Pharmaceutical Society of Japan
  • 摘要:Several kinds of absorbents, which were used for the determination of chlorine in the air by the pyridine·pyrazolone method, were investigated. Among p-toluenesulfonamide, sulfamic acid, 5, 5-dimethylhydantoin, isocyanuric acid and succinimide, only p-toluenesulfonamide was useful for the absorbent ; the others were useless because of a consumption of chlorine, a slow formation velocity of cyanogen chloride or an instability of chlorine. Furthermore, most of commercial potassium cyanides, which were also used for the determination method, were found to contain a reducing impurity. The impurity was a sulfite ion, and its content ranged from 100μg to 1400μg per 1 g of each potassium cyanide tested.
  • 关键词:chlorine;air;absorbent;p-toluenesulfonamide;potassium cyanide;reducing impurity;sulfite ion;cyanogen chloride;pyridine·pyrazolone reagent
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