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  • 标题:新規自動前処理装置を用いた食品中の動物用医薬品一斉分析法の妥当性確認
  • 作者:Yoichi YATSUKAWA ; Daisuke KUSUNO ; Takahiro MATSUDA
  • 期刊名称:食品衛生学雑誌
  • 印刷版ISSN:0015-6426
  • 电子版ISSN:1882-1006
  • 卷号:58
  • 期号:4
  • 页码:205-219
  • DOI:10.3358/shokueishi.58.205
  • 出版社:The Food Hygienic Society of Japan
  • 摘要:New automatic pretreatment equipment (FASVED; Food Automatic Analytical Systems for Veterinary Drugs) was developed. FASVED consists of ten main units: reagent dispenser, homogenizer, transfer hand, lid opening/closing device, centrifugal separator, pipette, shaker, column purification device, centrifugal evaporator and cooling device, and it is capable of freely combining operations by these units. A validation study was performed on two methods for determination of 178 veterinary drugs in livestock products, swine muscle, egg and shrimp, according to the method validation guideline of the Ministry of Health, Labour and Welfare of Japan. The numbers of analytes that satisfied the criteria of the guideline were 148 in swine muscle, 160 in egg and 151 in shrimp.
  • 关键词:automatic pretreatment equipment ; veterinary drug ; LC-MS/MS ; validation
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