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  • 标题:Preliminary results for the detection method of perfluoroalkyl substances (PFASs) residues in pork
  • 本地全文:下载
  • 作者:Shih-kuo Lin ; Maria Nobile ; Luca Chiesa
  • 期刊名称:International Journal of Health, Animal Science and Food Safety
  • 印刷版ISSN:2283-3927
  • 出版年度:2017
  • 卷号:4
  • 期号:1s
  • 语种:English
  • 出版社:Department of Health, Animal Science and Food Safety (VESPA)
  • 摘要:The perfluoroalkyl substances (PFASs) residues, which come from environmental pollution, tend to accumulate in the food chain (EFSA, 2008; Guerranti et al., 2013). 17 chemicals of PFASs family were selected for this study. Fresh pork samples were extracted by Waters ® WAX SPE (solid phase extraction) cartridges. All extracted samples were analyzed by liquid chromatography tandem mass spectrometry (LC-MS/MS). The results of calibration curves of each PFAS were good, the R 2 values ranging from 0.9901 to 0.9993. The Recoveries were in the range 80%-119%. The protocol of extraction by Waters ® WAX SPE cartridge will be applied in future studies.
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