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  • 标题:Simple synthesis of NH2-functionalized Fe2O3 and its activated carbon composites for removing heavy metal ions
  • 作者:C. L. Zhang ; H. D. Cheng ; S. Y. Ren
  • 期刊名称:IOP Conference Series: Earth and Environmental Science
  • 印刷版ISSN:1755-1307
  • 电子版ISSN:1755-1315
  • 出版年度:2018
  • 卷号:199
  • 期号:5
  • 页码:052042
  • DOI:10.1088/1755-1315/199/5/052042
  • 语种:English
  • 出版社:IOP Publishing
  • 摘要:The novel recyclable and biodegradable absorbents NH2-Fe2O3 and NH2-Fe2O3/oxidation-activated carbon (NH2-Fe2O3/OAC) with great physical properties and high adsorption for uptake heavy metal ions were synthesized in this work. The NH2-Fe2O3 samples were prepared via one-pot hydrothermal methods, typically, FeCl3 6H2O, ethylene glycol and sodium acetate anhydrous were directly dissolved under stirring, followed by x mL of DETA and 0.1 g of SDS at room temperature (x = 0.5, 1, 2, 3, 4 and 5 mL). The as-prepared NH2-Fe2O3 were added into the mixture of oxidation-activated carbon, followed by the cation surfactant CTAB. After reflux condensation, the composites were washed, dried and labeled name NH2-Fe2O3/OAC. Systematically characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), Fourier transform infrared spectra (FTIR) and X-ray diffraction (XRD), physicochemical properties were all indicated obviously in this paper. The high adsorption rates of the adsorbents achieved over 88.11 % and 98.25 % towards Pb(II). In the ternary solution, the studied heavy metals revealed selective removal sequence: Pb(II) > Cu(II) > Cd(II).
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