Tribological testing of polymeric material.
Kubatova, Dana ; Melichar, Martin ; Pereira, Alejandro 等
Tribological testing of polymeric material.
1. Introduction
In the technical, social and natural fields science there are many
unresolved issues and problems that scientists are looking for the
answers to, either in the form of answers at the theoretical level or in
practical application. After a period of massive development of R&D
during the last century, when energy efficiency and environmental
protection was not often considered, over the last few decades, and in
the third millennium, there has come a sobering awareness of the need to
save all kinds of energy. This is occurring against the background of
expansion and development of many disciplines relating to the quality of
human life, human needs and the desire to discover.
To fulfil these goals today machine and system builders should be
equipped with fairly deep knowledge of many disciplines. This
information enables them to solve problems in many areas. [1]
Situation in the field of durability and wear of machine parts
exposed to friction and wear is completely different. In many cases the
designers do not have necessary knowledge and technical documentation
about this. The problem stems primarily from the complexity interaction
of the materials on the functional surface machine components, the
variability of the operating conditions, which are determined by the
dominant factors that are friction and wear. Particularly when is
contact between moving parts metal on metal or a metal of an alternative
material, such as e.g.: polymer.
2. Polymeric material
Polymeric materials are basically divided according to their
properties for elastomers, thermoplastics and thermosets. For this test
were selected samples from polymeric materials in the field of
thermoplastics.
* AKRYLONITRILBUTADIENSTYREN next only ABS
* POLYAMID 6.6 with 15% GLASS FIBRE next only PA6.6+15%
* POLYAMID 6.6 next PA 6.6
* POLYAMID 6.6 with 30% GLASS FIEBRES
Note: bold materials were tested
Why polymeric materials? The answer is simple, because since the
time they were discovered, the man is trying various uses. Replace them
other materials, which have either limited or a polymer with its
specific characteristics surpass. Properties that polymeric materials
over conventional materials are numerous. Among the most interesting,
which make the polymers used are:
* Lightweight
* Electrical insulation properties
* Low thermal conductivity
* Corrosion Resistance
* Resistance to certain chemicals
* Flexibility / elasticity
* High fatigue resistance
* Resistance to aging
3. Sample
3.1. Preparation sample
For preparation samples was choosen method of injection moulding.
Injection was performed on machine Engel Victory 28 that is in
industrial laboratories of the University of Vigo.
The samples are in the form of a disc that have diameter [empty
set] 60 mm and a height of 3 mm. Sample size was chosen with regard to
the area to carry out all the tests, such as the repeated test
tribometer, roughness measurements and other tests.
Parameters for injection were set according to the parameters
provided by the manufacturer of the machine. The parameters used for
injection are seeing in Table 1 and 2. As a variable parameter was
chosen injection pressure in Table 2 marked yellow. These conditions
were the same for both materials tested.
Furthermore, the material PA6.6 + 15% GF was dryed before injecting
material. Drying was carried out at 80[degrees] C for 10 hours.
3.2. Testing of sample
Own tests selected plastic materials were conducted in cooperation
of Metrology lab of University of West Bohemia in Pilsen and
Laboratories University of Vigo.
This article partly describes preliminary tests. However, in this
article we have already come into field of repeated tests. Because it
was funded interesting information during the design of maps wear.
3.3. Tribological tests
The variability of this test allows exploring the different
possibilities of test materials. Tribotest setting options are almost
limitless.
The task of tribology is description of materials behaviour in a
relative motion. Tribology tested two or more materials in contact, or
interaction of the material with the environment there is a loss of
material from the surface, a process known as wear. The conditions used
in the tests are shown in Table 3.
4. Friction coefficient
4.1. ABS material
This parameter is the most important value for this test. On the
basis of information about the value of the friction coefficient, one is
able to predict how the material will behave under load. Thus, both will
be wearing, how will heat up or how it will deform ...
The parameter is measured during continuous tribological testing
and then this value continues to operate. This test measured the
coefficient of friction for long term testing since the objective was to
determine the mean coefficient of friction.
Label groups:
* 1-150 bar and roughness poor
* 2-100 bar and roughness poor
* 3-100 bar and roughness good
* 4-150 bar and a roughness good
The upward trend of the coefficient of friction is due to the fact
that they still rises contact area when pike test specimen and the test
sample.
In Fig. 1, graph 200rpm and 20N in Category 3 (gray line) shows a
decreasing tendency from the value of 70% and is probably due to a
problem in the structure of the sample.
Furthermore, this test confirmed that the friction coefficient
depends on the value of surface roughness, as shown Fig. 1 in the
following figures and example. At 200 rpm and a load of 30 N it has the
best surface roughness of the sample group which has poor roughness.
For better orientation, the effect of the load value, and scanning
speed (time) is shown in the following Fig. 2 and 3..
It is easy to see how changes the value of the coefficient of
friction changes for each load and speed testing. It is seen that the
coefficient decreases with increasing load and speed combination
testing.
4.2. Polyamide material
Even for this material, comparisons were made between the loads for
the groups as in the previous tests. However, for these comparisons
nothing unusual was found, therefore only the resulting comparison is
given.
This comparison is interesting in that the greatest friction
coefficient was achieved at maximum load. This can be anything from
previous tests to explain why it is necessary to carry out further tests
with those conditions and that both the load and speed of rotation but
also the same moisture conditions. Moisture is needed in this case the
guard due to the fact that PA6.6 + 15% GF is a highly hygroscopic
material.
5. Change of weight
The changing weight of the sample describes how much the research
sample wears under the influence of higher pressure and cyclic effect
(rotary) wear.
Here, in the graph for PA6.6 + 15% GF it is important to note that
we changed the mass immediately after injection of the sample and before
the test. This is due to the very high hygroscopicity material.
From Chart 3 it is already possible to say how the material will
behave during further testing and what results can be expected from
additional tests, and that material PA 6.6 + 15%GF will better withstand
potential stresses than ABS. In numbers, this is expressed by ABS during
the test, lost 0.017ga PA 6.6 + 15%GF lost 0.003 g.
6. Wear map
Wear maps describes how material will behave in the area of tested
conditions. Maps are used to get quickly information about the material.
Maps are use not only for getting behaviour but the maps are used for
comparing two or more of the tested materials and on how they are
against each other position of their mechanical properties. However, all
this can be expected only if the tests are carried out under the same
test conditions--the same testing body, our case was used steel ball
diametre 4 mm and test conditions see Table 3.
For construct a wear maps is necessary to know the width, depth and
average diameter traces left at sample after the test tribometer.
To determine the actual width tracks and medium diameter traces
were used a microscope connected to a pc in the laboratories of the
University of Vigo. Images from this measurement can be seen in Fig. 8.
The microscope was set lens 10x zoom 1x.
As an additional parameter is the depth of left traces. This was
measured in Laboratories University of West Bohemia device to Etamic
Hommel T8000. Device enables to measure both the profile and roughness
of components. There was used the profile measurement. The output from
the measuring is seeing on Fig. 9. The red box in Fig. 9 is marked path
area after tribotest.
After obtaining all the parameters necessary for calculating the
wear map has been calculated to obtain data for constructing and plotted
into a graph that can be seen in Fig. 10.
Usually wear maps are constructed only of individual points.
However, when is given two or more materials into one wear maps is
difficult to orientation in this map. Therefore in this case is map
completed by connecting lines, which enable easier orientation in the
chart.
7. Conclusion
ABS and PA are polymers and are thermoplastics. Therefore, they
should have roughly the same properties and characteristics as some
specific parameters for these materials.
Even in terms of comfort for the test were as arm Vibration noise
or better based material PA6.6 + 15% GF.
In the article non-traditional is map designed for wear two
materials together. Here the article being wear value related to the
ratio of modulus of elasticity. The modulus of elasticity was chosen
because it clearly defines the internal structure of the material.
Assumption was that for the same test parameters (conditions tribotestu)
should result in less wear on the material with higher modulus of
elasticity. This hypothesis was confirmed, but not the value of the
wear. The wear values could according modulus should differ by about
70%. While the wear values differ by more than 90%.
If the resultant product is used as an exposed part, according to
the test the clear choice is ABS. This is covered by acquired better
visual structures and surface roughness, and after averaging all values
amino slightly smaller friction coefficient than PA66 + 15% GF.
However, when used as a loaded component, this material is very
difficult to use. Large wear loss of material occurs when loading, which
is adhered in the form of fine dust on all around visibility
DOI: 10.2507/27th.daaam.proceedings.063
8. Acknowledgment
The present contribution has been prepared under project LO1502
'Development of the Regional Technological Institute' under
the auspices of the National Sustainability Programme I of the Ministry
of Education of the Czech Republic aimed to support research,
experimental development and innovation.
9. References
[1] M. Renouf, F. Massi, N. Fillot, A. Saulot, Numerical tribology
of a dry contact, Tribology International, Volume 44, Issues 7-8, July
2011, Pages 834-844, ISSN 0301-679X,
http://dx.doi.org/10.1016/j.triboint.2011.02.008
[2] T. Mathia, P. Pawlus y M. Wieczorowski, <<Recent trends
in surface metrology,>> Wear, p. 494-508, 2011
[3] D. Kubatova, M. Melichar, A. Pereira, Comparative Study of
Tribological Behaviour of Polyamide and Abs Polymers After Processing by
Injection
[4] J. Sudeepan, K. Kumar, T.K. Barman, P. Sahoo, Study of Friction
and Wear of ABS/Zno Polymer Composite Using Taguchi Technique, Procedia
Materials Science, Volume 6, 2014, Pages 391-400, ISSN 2211-8128,
http://dx.doi.org/10.1016Zj.mspro.2014.07.050
[5] ASM handbook. 10th editon. Materials Park, Ohio: ASM
International, 2016. ISBN 1615038272
This Publication has to be referred as: Kubatova, D[ana]; Melichar,
M[artin] & Pereira, A[lejandro] (2016). Tribological Testing of
Polymeric Material, Proceedings of the 27th DAAAM International
Symposium, pp.0428-0434, B. Katalinic (Ed.), Published by DAAAM
International, ISBN 978-3-902734-08-2, ISSN 1726-9679, Vienna, Austria
Caption: Fig. 1 Friction coefficient during testing for ABS
material--according to the test parameters
Caption: Fig. 2 Friction coefficient--ABS material summarization
Caption: Fig. 3 Friction coefficient--ABS material summarization
Caption: Fig. 4 Friction coefficient--comparison ABS and PA6,6+15%
GF
Caption: Fig. 5 Differences between weights for ABS material
Caption: Fig. 6 Differences between weights for PA material
Caption: Fig. 7 Comparison ABS and PA material--weights lost
Caption: Fig. 8 Measuring stops after testing--width and radius
Caption: Fig. 9 Measuring stops after testing--deep
Caption: Fig. 10 Wear map for two materials
Table 1. Temperature during injection
Set max. Temperature 265 255 240 220
in the cylinders /[degrees]C/
The actual temperature 249,7 249,5 239,7 220
in the cylinder /[degrees]C/
Set max. Temperature 40
in the cylinders /[degrees]C/
The actual temperature 45,7
in the cylinder /[degrees]C/
Table 2. Injection parameters
Injection volume 17 cm3 17 cm3
Max. pressure 160 bar 160 bar
Piston diameter 30 mm 30 mm
Time injection 2 s 2 s
Cooling time in the form of 20 s 20 s
Injection pressure 100 bar 150 bar
Volume of the mould 11 cm3 11 m3
Table 3. Testing parameters
Material Speed test Radiu test Load Time test
/rpm/ /mm/ /N/ /m/
ABS-1-a 200 9 20 200
ABS-1-b
ABS-2-a
ABS-2-b 300 30
PA-1-a
PA-2-a
Radius test
bodies
Material /mm/
ABS-1-a 4
ABS-1-b
ABS-2-a
ABS-2-b
PA-1-a
PA-2-a
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