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  • 标题:Cyclic Sulfamidite as Simultaneous Protecting Group for Amino Alcohols: Development of a Mild Deprotection Protocol Using Thiophenol
  • 本地全文:下载
  • 作者:Juri Sakata ; Kazunari Akita ; Manabu Sato
  • 期刊名称:Chemical and Pharmaceutical Bulletin
  • 印刷版ISSN:0009-2363
  • 电子版ISSN:1347-5223
  • 出版年度:2020
  • 卷号:68
  • 期号:10
  • 页码:996-1000
  • DOI:10.1248/cpb.c20-00531
  • 出版社:The Pharmaceutical Society of Japan
  • 摘要:

    This study describes the novel utility of cyclic sulfamidite as a simultaneous protecting group for 1,2- or 1,3-amino alcohols. An exceptionally mild and neutral condition for the removal of the cyclic sulfamidite was developed. The deprotection condition demonstrated a broad range of functional-group compatibility, including a substrate bearing a Z -enyne structure without any loss of double-bond stereochemistry.

  • 关键词:protecting group;amino alcohol;protection;deprotection;cyclic sulfamidite
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