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  • 标题:Investigation of Magnetic and Optical Properties of Mn-Doped SnO 2 at Different Annealing Temperatures
  • 本地全文:下载
  • 作者:S. Negi ; A. Sharma ; P. Sharma
  • 期刊名称:Journal of Scientific Research
  • 印刷版ISSN:2070-0237
  • 电子版ISSN:2070-0245
  • 出版年度:2020
  • 卷号:12
  • 期号:4
  • 页码:555-567
  • DOI:10.3329/jsr.v12i4.46052
  • 出版社:Rajshahi University
  • 摘要:In this paper, a systematic investigation has been done to study the effect of variation in annealing temperature on magnetic and optical properties of Mn-doped SnO2. Co-precipitation technique has been used to synthesize Sn1-xMnxO2 samples with low Mn concentration (2 %). Pristine SnO2 is sintered at 350 oC. Mn-doped SnO2 samples are sintered at 350, 450, 550 and 650 oC. The structures of tetragonal rutile of SnO2 and Mn-doped SnO2 have been confirmed by the XRD pattern. Typical ferromagnetic ordering has been observed for Mn-doped SnO2 samples annealed at different temperatures. However, on increasing the annealing temperature saturation magnetization as well as the coercive field decreases, indicating a crucial phase transformation from ferromagnetism to paramagnetism. UV-Vis spectroscopy shows increase in absorbance and a slight shift in the absorption edge with Mn-doping at increasing annealing temperature indicating shifting of absorption peak towards higher wavelength. Tauc’s plot has been used to find the optical band gap (Eg).
  • 关键词:Annealing temperature; Co-precipitation; X-ray diffraction; Energy band gap.
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