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  • 标题:Fabrication of redispersible silica nanoparticles by a facile one-step one-pot approach
  • 本地全文:下载
  • 作者:Haitao Liu ; Hailin Cao ; Yudong Huang
  • 期刊名称:E3S Web of Conferences
  • 印刷版ISSN:2267-1242
  • 电子版ISSN:2267-1242
  • 出版年度:2020
  • 卷号:213
  • 页码:1-5
  • DOI:10.1051/e3sconf/202021301018
  • 出版社:EDP Sciences
  • 摘要:In this study, special redispersible silica nanoparticles (SNP) was synthesized by a facile one-step one-pot approach. The synthesized amorphous SNP had a spherical and uniform particle morphology with a diameter of 30 nm and exhibited high monodispersity. The characteristics of the particles were investigated by fourier transform infrared spectroscopy and thermogravimetric analysis. The results revealed that there were a large number of methyl groups grafted on the surface of the SNP, and the organic materials content in the as-synthesized SNP was approximately 10%. After a simple ultrasonic process, the SNP solid powder showed excellent stable and transparent redispersion in various organic solvents. In addition, the results revealed that the different polarities of the solvents had a significant effect on the visible light transparency of the SNP redispersion. SNP showed the best redispersion performance in N-methyl-pyrrolidone, exhibiting a transmittance of more than 80% at 600 nm at a high concentration of 25 wt%. The synthesis process developed in this study is simple, inexpensive, and can be used in the industrial application of SNP.
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