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  • 标题:Synthesis and Characterization of Zeolitic Imidazolate Framework-8 (ZIF-8)/Al2O3 Composite
  • 本地全文:下载
  • 作者:Wulan Aulia ; Ahnaf Ahnaf ; Mochammad Yusuf Irianto
  • 期刊名称:Majalah Iptek = IPTEK : The Journal for Technology and Science
  • 印刷版ISSN:0853-4098
  • 电子版ISSN:2088-2033
  • 出版年度:2020
  • 卷号:31
  • 期号:1
  • 页码:18-24
  • DOI:10.12962/j20882033.v31i1.5511
  • 出版社:IPTEK
  • 摘要:Metal-organic framework (MOF) such as ZIF-8 is the tremendous porous material applied in many fields due to high specific surface area and excellent regularity of pores. One technique to improve the physical properties of ZIF-8 with the formation of a composite between a metal oxide and MOF. ZIF-8 and ZIF-8/퐴푙2푂3 were successfully synthesized by the solvothermal method with an 퐴푙 variation of 19%, 38%, and 76%. The ZIF-8/퐴푙2푂3 were characterized by XRD, FTIR, SEM, and 푁2 Physisorption. The diffractogram shows that the appearing of ZIF-8’s peak on 2θ = 7.26; 10.41, 12.66, 16.41, and 17.95°. The morphological of ZIF-8 crystals had a cubic shape. Then the ZIF-8/퐴푙2푂3 had different shapes with ZIF-8. Based on the FTIR result, the Zn-N peak appears on 420 푐푚−1, which indicates the bonding between metal and organic ligand for ZIF-8/퐴푙2푂3 has an additional spike on 825 푐푚−1 due to the vibration of 퐴푙 − 푂 − 퐴푙.
  • 关键词:Synthesis; ZIF-8; Al2O3; Metal-Organic Framework
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