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  • 标题:An Optical and Structural Study of Pentacene Thin-film Polymorphs
  • 本地全文:下载
  • 作者:Franklin Wong ; Rui He ; Aaron Pinczuk
  • 期刊名称:Columbia Undergraduate Science Journal
  • 印刷版ISSN:1932-765X
  • 电子版ISSN:1932-7641
  • 出版年度:2006
  • 卷号:1
  • 期号:1
  • 出版社:Columbia Undergraduate Science Journal
  • 摘要:

    Because of its high conductivity, pentacene is an attractive organic material for electronic applications, but the understanding of its thin-film polymporphism is still lacking. In this work, two pentacene films, 70nm and 2.5µm thick, were evaporated onto silicon dioxide substrates. X-ray Diffraction identified two different phases in the 70nm film and four in the 2.5µm film. Oxygen and fluorine impurities were detected by X-ray Photoelectron Spectroscopy, suggesting that some of the phases in the films may be impurity-based mixed crystals of pentacene. With improved sensitivity from the resonance Raman effect, low-energy intermolecular phonons were studied and assigned as signature modes to the different polymorphs identified in the films. The 39cm-1 mode is characteristic of the 14.3Å pure pentacene polymorph, and the 45 and 50cm-1 modes are signatures of the 15.3Å pure polymorph. This is the first time that the intermolecular modes of pentacene thin films has been studied, and a more thorough analysis can further elucidate the structures of the different thin-film polymorphs.

  • 关键词:Structural Studies,Organic Material,Electronic Applications,Pentacene Films,X-Ray Photoelectron Spectroscopy,Resonance Raman Effect,Pentacene Polymorphs
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