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  • 标题:A Convenient Method for the Synthesis of Bis-Ureas Using Bis(O-Nitrophenyl) Carbonate as Starting Material
  • 本地全文:下载
  • 作者:M.C. Turoczi ; M. Simon ; C. Csunderlik
  • 期刊名称:Universitatea Politehnica din Timisoara. Buletinul Stiintific. Seria Chimie si Ingineria Mediului
  • 印刷版ISSN:1224-6018
  • 出版年度:2007
  • 卷号:52(66)
  • 期号:01-02
  • 出版社:Universitatea Politehnica din Timisoara
  • 摘要:A general method for the preparation of bis-ureas from bis(o-nitrophenyl)carbonate have been developed. Directional urea synthesis is achieved by sequential amine addtition to bis(o-nitrophenyl)carbonate in two steps: as a first step bis(o-nitrophenil) carbonate is reacted with benzyl amine to form benzyl-o-nitrophenyl carbamate; in the second step the carbamate is reacted with a variety of diamines in toluen to yield bis-ureas.
  • 关键词:bis(o-nitrophenyl) carbonate, carbamate, bis-urea
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