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  • 标题:Synthesis, NMR and Single Crystal analysis of Novel 2,9-dimethyl-4,7-diphenyl[1,10]phenanthrolinediium,
  • 本地全文:下载
  • 作者:Warad I. ; Haddad S.F. ; Al-Noaimi M.
  • 期刊名称:Journal of Materials and Environmental Science
  • 印刷版ISSN:2028-2508
  • 出版年度:2014
  • 卷号:5
  • 期号:2
  • 页码:470-475
  • 出版社:University of Mohammed Premier Oujda
  • 摘要:2,9-dimethyl -4,7 -diphenyl[1,10]phenanthrolinediium was made available by acidifying of 2,9-dimethyl-4,7-diphenyl-1,10-phenanthroline in ethanol solvent using conc. HCl as acid. The bi-protonation of pyridine in phenanthroline was mo nitored by 1H NMR and confirmed by X-ray single crystal, X RD structure of desired product was found to be a Monoclinic crystal system with C2/c1 space group and Z = 6
  • 关键词:Phenanthrolinediium; phenanthroline ligand; NMR; XRD
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